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工程科学与技术:2017,49(Z2):244-250
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两种电场快速烧结方法制备W-Cu合金的对比研究 “研究生论坛”稿件,投稿栏目为“研究生论坛”
(四川大学制造科学与工程学院)
Comparative Study on the Rapid Sintering of W-Cu alloy under the action of two different electric fields
(School of Manufacturing Science and Engineer , Sichuan University)
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投稿时间:2016-09-02    修订日期:2017-03-22
中文摘要: 为了解决传统烧结方法制备W-Cu合金存在的烧结温度高、烧结时间长、晶粒长大严重等缺点,利用电场对材料烧结的促进作用,本文采用放电等离子烧结(SPS)和大电流电阻烧结两种电场快速烧结方法制备W-Cu合金。借助阿基米德排水法测量密度和金相显微镜、扫描电镜等分析测试方法,对两种电场快速烧结方法在不同烧结温度条件下(800℃、900℃、1000℃)制备的W-20wt%Cu合金的致密化程度及显微组织结构进行了对比研究。通过对两种烧结方法中电场密度的计算和烧结体显微组织结构中铜池的出现,结果表明:在本实验条件下,相比放电等离子烧结法,采用大电流电阻烧结法在加热过程中更容易产生场致发射效应,这有利于W-Cu合金组织的均匀分布,促进烧结致密化。大电流电阻烧结体的相对密度和显微组织结构均优于放电等离子烧结体;采用放电等离子烧结,烧结温度从800℃提高到900℃时,烧结体的相对密度增大,合金内部孔洞和晶粒的大小、分布更加均匀,但当烧结温度达到1000℃时,烧结体的相对密度增幅不大,烧结体孔洞集中,且晶粒团聚;而在大电流电阻烧结时,随着烧结温度升高,烧结体的相对密度增大,显微组织结构的均匀性也得到提高。
中文关键词: 电场  快速烧结  W-Cu合金
Abstract:In order to solve the shortcomings such as high sintering temperature, long sintering time and severe grain growth in the preparation of W-Cu alloy by traditional sintering technologies, W-Cu alloy was rapidly sintered by spark plasma sintering (SPS) and large current resistance sintering under an electric field which promoted the sintering process. With the help of Archimedes drainage method, metallographic microscope and scanning electron microscope etc., the densification degree and microstructure of W-20wt%Cu alloy prepared by two kinds of electric field rapid sintering methods at different sintering temperature (800℃, 900℃, and 1000℃) were studied.Through the calculation of the electric field density in two sintering methods and the appearance of the copper pool in the microstructure, the results showed that: large current resistance sintering was more likely to have a field emission effect compared with SPS, this was favorable for the microstructure and densification of W-Cu alloy. Samples sintered under large current resistance?possessed higher relative density and more?homogeneous microstructure, in?comparison to?samples from?SPS. In spark plasma sintering, the relative density of sintered samples increased and the uniformity of microstructure improved with the sintering temperature increased from 800℃ to 900℃; while concentration distribution of holes and aggregation of particles could be seen in sample sintered at 1000℃. However, the relative density of sintered samples obtained under large current resistance sintering increased and the uniformity of microstructure improved with the sintering temperature raising.
文章编号:201600924     中图分类号:    文献标志码:
基金项目:“W-Mo-Cu复合材料优化设计及其电场快速烧结的基础研究”(国家自然科学基金面上项目,编号:51674171)
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引用文本:
周虹伶,冯可芹.两种电场快速烧结方法制备W-Cu合金的对比研究 “研究生论坛”稿件,投稿栏目为“研究生论坛”[J].工程科学与技术,2017,49(Z2):244-250.
ZHOU Hongling,FENG Keqin.Comparative Study on the Rapid Sintering of W-Cu alloy under the action of two different electric fields[J].Advanced Engineering Sciences,2017,49(Z2):244-250.